Basic Gas Chromatography by James M. Miller (English) Hardcover Book

Description: Basic Gas Chromatography by James M. Miller, Nicholas H. Snow, Harold M. McNair Basic Gas Chromatography, Third Edition provides a brief introduction to GC following the objectives for titles in this series. It should appeal to readers with varying levels of education and emphasizes a practical, applied approach to the subject. : This book provides a quick need-to-know introduction to gas chromatography; still the most widely used instrumental analysis technique, and is intended to assist new users in gaining understanding quickly and as a quick reference for experienced users. The new edition provides updated chapters that reflect changes in technology and methodology, especially sample preparation, detectors and multidimensional chromatography. The book also covers new detectors recently introduced and sample preparation methods that have become much more easily accessible since the previous edition. FORMAT Hardcover LANGUAGE English CONDITION Brand New Back Cover Provides a quick, yet comprehensive, need-to-know introduction to gas chromatography This new edition of Basic Gas Chromatography provides a brief introduction to GC, which is still the most widely used instrumental analysis technique today. It includes updated chapters that reflect changes in technology and methodology, especially sample preparation, detectors, and multidimensional chromatography. In addition, the book also covers recently introduced detectors and sample preparation methods that have become much more easily accessible since the previous edition. Basic Gas Chromatography, Third Edition covers the latest in the field, giving readers the most up-to-date guide available, while maintaining the previous editions practical, applied approach to the subject and its accessibility to a wide range of readers. Inside, readers will find complete coverage of basic topics in the field--such as stationary phases, capillary columns, packed columns, inlets, detectors, and qualitative and quantitative analysis. Theyll also discover chapters on gas chromatography-mass spectrometry (GC-MS); sampling methods; multidimensional gas chromatography and introductions to fast gas chromatography; gas chromatography analysis of nonvolatile compounds; and inverse and pyrolysis gas chromatography. Concise and fundamental in its coverage of gas chromatography Updated with the latest changes in technology and methodology, including sample preparation, detectors, and multidimensional chromatography Offers revised references, resources, and Web sites that reflect the state of the field Covers the most current detectors and sample preparation methods A handy reference for experienced users and an excellent book for new readers who need to get up to speed fast Basic Gas Chromatography, Third Edition remains the standard handbook for everyone from undergraduates studying analytical chemistry to working industrial chemists. Flap Provides a quick, yet comprehensive, need-to-know introduction to gas chromatography This new edition of Basic Gas Chromatography provides a brief introduction to GC, which is still the most widely used instrumental analysis technique today. It includes updated chapters that reflect changes in technology and methodology, especially sample preparation, detectors, and multidimensional chromatography. In addition, the book also covers recently introduced detectors and sample preparation methods that have become much more easily accessible since the previous edition. Basic Gas Chromatography, Third Edition covers the latest in the field, giving readers the most up-to-date guide available, while maintaining the previous editions practical, applied approach to the subject and its accessibility to a wide range of readers. Inside, readers will find complete coverage of basic topics in the field--such as stationary phases, capillary columns, packed columns, inlets, detectors, and qualitative and quantitative analysis. Theyll also discover chapters on gas chromatography-mass spectrometry (GC-MS); sampling methods; multidimensional gas chromatography and introductions to fast gas chromatography; gas chromatography analysis of nonvolatile compounds; and inverse and pyrolysis gas chromatography. Concise and fundamental in its coverage of gas chromatography Updated with the latest changes in technology and methodology, including sample preparation, detectors, and multidimensional chromatography Offers revised references, resources, and Web sites that reflect the state of the field Covers the most current detectors and sample preparation methods A handy reference for experienced users and an excellent book for new readers who need to get up to speed fast Basic Gas Chromatography, Third Edition remains the standard handbook for everyone from undergraduates studying analytical chemistry to working industrial chemists. Author Biography HAROLD M. MCNAIR, PHD, is Professor Emeritus of Chemistry at Virginia Tech, and is known internationally as a leading researcher and educator in the field of gas chromatography. JAMES M. MILLER, PHD, is Professor Emeritus of Chemistry at Drew University, where he taught for 36 years. NICHOLAS H. SNOW, PHD, is Professor of Chemistry and Biochemistry at Seton Hall University. He is widely published in gas chromatography and has been teaching GC to new students for over 30 years. Table of Contents Preface to the Third Edition xi Preface to the Second Edition xiii Preface to the First Edition xv Acknowledgments xvii 1 Introduction 1 A Brief History 1 Definitions 3 Overview: Advantages and Disadvantages 9 Instrumentation and Columns 12 References 14 2 Basic Concepts and Terms 15 Definitions, Terms, and Symbols 15 The Rate Theory 25 The Achievement of Separation 34 References 35 3 Instrument Overview 37 Carrier Gas 38 Flow Control and Measurement 39 Sample Inlets and Sampling Devices 42 Capillary Columns 46 Temperature Zones 47 Detectors 49 Data Systems 50 Reference 50 4 Capillary Columns 51 Types of Capillary Columns 51 Capillary Column Tubing 54 Advantages of Capillary Columns 55 Column Selection 57 Column Quality Testing: The Grob Test Mix 65 Special Troubleshooting Considerations for Capillary Columns 66 Guidelines for Selecting Capillary Columns 67 References 68 5 Stationary Phases 69 Selecting a Column 69 Common and Important Stationary Phases 81 Other Common Stationary Phases 83 References 86 6 Temperature Programming 87 Advantages and Disadvantages of TPGC 89 Requirements for TPGC 90 Example Temperature Programmed Chromatograms 91 Special Topics 96 References 98 7 Inlets 99 Inlet Fundamentals 99 Split Inlet 101 Splitless Inlet 104 OnColumn Inlet 106 Programmed Temperature Vaporizer (PTV) 107 Related Topics 108 References 111 8 Classical Detectors: FID, TCD, and ECD 113 Classification of Detectors 115 Common Detector Characteristics 117 Flame Ionization Detector (FID) 124 Thermal Conductivity Detector (TCD) 128 Electron Capture Detector (ECD) 131 Other Detectors 134 References 136 9 Qualitative and Quantitative Analysis 139 Qualitative Analysis 139 Quantitative Analysis 145 Statistics of Quantitative Calculations 145 Quantitative Analysis Methods 148 Summary 154 References 154 10 GCMS and Spectrometric Detectors 157 Gas Chromatography–Mass Spectrometry (GCMS) 158 Gas Chromatography–Mass Spectrometry–Mass Spectrometry (GCMSMS) 171 Gas Chromatography–Fourier Transform Infrared Spectrometry (GCFITR) 172 Gas Chromatography–Vacuum Ultraviolet (GCVUV) Spectrometry 172 References 174 11 Sampling Methods 177 Overview 177 Liquid–Liquid Extraction (LLE) 179 Solid–Liquid Extraction: Soxhlet Extraction and Accelerated Solvent Extraction (ASE) 182 SolidPhase Extraction 183 Liquid–Vapor or Solid–Vapor Extraction: Headspace Extraction 186 Solid-phase microextraction (SPME) 188 QuEChERS (Quick, Easy Cheap, Effective, Rugged, Safe) 192 Additional Techniques and Summary 193 References 194 12 Multidimensional Gas Chromatography 197 Overview 197 Fundamental Principles of Multidimensional Chromatography 198 Heart Cutting 202 Comprehensive TwoDimensional GC (GC×GC) 203 LCGC with Heart Cutting 206 Comprehensive LC×GC 206 References 208 13 Packed Column GC 211 Columns 211 Solid Supports and Stationary Phases 213 Liquid Stationary Phases 214 Solid Stationary Phases 215 Gas Analysis 218 Analysis of Other Inorganics 221 Inlets and Liquid Sampling for Packed Columns 221 Special Columns and Applications 222 References 224 14 Special Topics 225 Fast GC 225 Chiral Analysis by GC 228 Analysis of Nonvolatile Compounds 229 Pyrolysis 233 Inverse GC 233 Additional Theory 234 Activity Coefficients 236 References 238 15 Troubleshooting GC Systems 241 Preventing Problems 241 Troubleshooting Problems 243 Appendix A Acronyms, Symbols and Greek Symbols 251 Appendix B Some Internet Sites for Gas Chromatography 255 Appendix C Other Books On Gas Chromatography 257 Index 259 Details ISBN1119450756 Year 2019 ISBN-10 1119450756 ISBN-13 9781119450757 Format Hardcover Edition 3rd Country of Publication United States DEWEY 543.85 Pages 288 Language English Publication Date 2019-09-27 UK Release Date 2019-09-27 Imprint John Wiley & Sons Inc Place of Publication New York AU Release Date 2019-08-06 NZ Release Date 2019-08-06 Author Harold M. McNair Publisher John Wiley & Sons Inc Edition Description 3rd edition Replaces 9780470439548 Audience Professional & Vocational US Release Date 2019-09-27 We've got this At The Nile, if you're looking for it, we've got it. With fast shipping, low prices, friendly service and well over a million items - you're bound to find what you want, at a price you'll love! TheNile_Item_ID:136207237;

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